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Synthesis Of ChloroformEssay Preview: Synthesis Of ChloroformReport this essaySynthesis of ChloroformWith Calcium Hypochlorite and AcetoneWhen chlorine is passed into boiling alcohol, both chlorination of the methyl group and oxidation of the primary alcohol group to an aldehyde occur, giving trichloro-acetaldehyde or chloral: When chloral is treated with caustic alkali, fission of the C-C linkage occurs,.