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Dihydroxylation of Cyclohexene Essay Preview: Dihydroxylation of Cyclohexene Report this essay Dihydroxylation of Cyclohexene Abstract This was a microscale experiment in which cyclohexane-1,2-diol was synthesized by dihydroxylation of cyclohexene. Oxone, a persulfate mix that reacts with acetone to produce dimethydioxirane, reacts with cyclohexene to form cyclohexane-1,2-diol. Through a thin layer chromatography (TLC) analysis, it was.