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Simple Distillation and Gas Chromatography Discussion Questions Alyssa Winborne10/19/14Ochem 237 Section 511Simple Distillation and Gas Chromatography Discussion QuestionsIn this experiment we learned how to purify volatile compounds by simple distillation and we learned how to use gas chromatography to quantitatively determine the relative proportions of volatile compounds in the samples we were given. Volatile compounds.