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Preparation of P-Nitroaniline from P-Nitroacetanilide Essay Preview: Preparation of P-Nitroaniline from P-Nitroacetanilide Report this essay Step 1: Acetylation of Aniline In the first step we need to put the removable acetyl protecting group on the nitrogen of aniline. The acetyl group is electron withdrawing and it therefore makes the lone pair on the nitrogen less.