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X-Ray Photoelectron Spectroscopy Essay Preview: X-Ray Photoelectron Spectroscopy Report this essay X-ray Photoelectron Spectroscopy – A Report I. Overview This report is a detailed study on X-ray Photoelectron Spectroscopy (XPS), a surface characterization technique. The first question that probably comes in your mind is, what exactly is surface characterization? Well, surface characterization is a method.